Guyana is about 4.8 times smaller than Mauritania.

Mauritania is approximately 1,030,700 sq km, while Guyana is approximately 214,969 sq km, making Guyana 20.86% the size of Mauritania. Meanwhile, the population of Mauritania is ~4.2 million people (3.4 million fewer people live in Guyana).
This to-scale comparison of Mauritania vs. Guyana uses the Mercator projection, which distorts the size of regions near the poles. Learn more.

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